The idea of the mass of matter was first shaped into an exact form by Galileo (died 1642), and more especially by Newton (born 1643, died 1727), in the glorious epoch of the development of the principles of inductive reasoning enunciated by Bacon and Descartes in their philosophical treatises. Shortly after the death of Newton, Lavoisier, whose fame in natural philosophy should rank with that of Galileo and Newton, was born on August 26, 1743. The death of Lavoisier occurred during the Reign of Terror of the French Revolution, when he, together with twenty-six other chief farmers of the revenue, was guillotined on May 8, 1794, at Paris; but his works and ideas have made him immortal.
By covering iron with an enamel, or varnish, or with unrustable metals (such as nickel), or a coating of paraffin, or other similar substances, it is protected from the air and moisture, and so kept from rusting.
Such an experiment may easily be made by taking the finest (unrusted) iron filings (ordinary filings must be first washed in ether, dried, and passed through a very fine sieve). The filings thus obtained are capable of burning directly in air (by oxidising or forming rust), especially when they hang (are attracted) on a magnet. A compact piece of iron does not burn in air, but spongy iron glows and smoulders like tinder. In making the experiment, a horse-shoe magnet is fixed, with the poles downwards, on one arm of a rather sensitive balance, and the iron filings are applied to the magnet (on a sheet of paper) so as to form a beard about the poles. The balance pan should be exactly under the filings on the magnet, in order that any which might fall from it should not alter the weight. The filings, having been weighed, are set light to by applying the flame of a candle; they easily take fire, and go on burning by themselves, forming rust. When the combustion is ended, it will be clear that the iron has increased in weight; from 5½ parts by weight of iron filings taken, there are obtained, by complete combustion, 7½ parts by weight of rust.
For the purpose of experiment, it is most convenient to take copper carbonate, which may be prepared by the experimenter himself, by adding a solution of sodium carbonate to a solution of copper sulphate. The precipitate (deposit) so formed is collected on a filter, washed, and dried. The decomposition of copper carbonate into copper oxide is effected by so moderate a heat that it may be performed in a glass vessel heated by a lamp. For this purpose a thin glass tube, closed at one end, and called a ‘test tube,’ may be employed, or else a vessel called a ‘retort.’ The experiment is carried on, as described in example three on p. 11, by collecting the carbonic anhydride over water, as will be afterwards explained.
Gas delivery tubes are usually made of glass tubing of various diameters and thicknesses. If of small diameter and thickness, a glass tube is easily bent by heating in a gas jet or the flame of a spirit lamp, and it may also be easily divided at a given point by making a deep scratch with a file and then breaking the tube at this point with a sharp jerk. These properties, together with their impermeability, transparency, hardness, and regularity of bore, render glass tubes most useful in experiments with gases. Naturally they might be replaced by straws, india-rubber, metallic, or other tubes, but these are more difficult to fix on to a vessel, and are not entirely impervious to gases. A glass gas delivery tube may be hermetically fixed into a vessel by fitting it into a perforated cork, which should be soft and free from flaws, and fixing the cork into the orifice of the vessel. To protect the cork from the action of gases it is sometimes previously soaked in paraffin, or it may be replaced by an india-rubber cork.